Experimental Trial Journal


This journal is a compilation of basic descriptions of the different tests that the group conducted on their heat pipe, as well as the results, what those results indicated to the group members, and the recorded data from each test organized in both charts and graphs.

Test #1: 20 mL Water in "Harold" the Heat Pipe Prototype
One of the first tests using the 15 psi gauge at the top and only one thermocoupling.
The first trial took place on Sunday morning April 24, 2016. The temperature of the heat pipe was at this point only being measured at one location, farther away from the initial heat source (hereafter also referred to as the far location). The temperature of the heat pipe at the far location remained stable at around room temperature for 1:30, before rising steadily. However, the pressure gauge remained stagnant, and group members realized that the valve from the heat pipe to the pressure gauge had been closed the night before had not re-opened in the morning. As a result, the recorded data was thrown out, and the trial re-started.

Test #2: 20 mL Water in "Harold" 
This was another faulty trial. In between each test, it was necessary to cool the pipe (and the heat transfer fluid within the pipe) back to room temperature. Part of this process involved opening a vent on the side of the heat gun. (Please keep in mind that it was still pretty early in the morning and the group had gone to bed only a handful of hours before) The temperature of the heat pipe was not rising, and within the first 45 seconds of the trial, the group members realized that the vent on the side of the heat pipe was still open. They closed it, erased the useless data, and began once again on their testing. 

Test #3: 20 mL Water in "Harold"
The third trial was a bit troubling, as all of the mechanisms were in the correct positions, but the results were less useful than those of the test conducted on Saturday night (before anyone started recording). The temperature climbed more slowly than expected, but the real struggle came in when the 15 psi pressure gauge was maxed out within the first 3 minutes. The group decided that 15 psi was not enough to measure the pressure up to, so switched the gauge for one that maxed out at 30 psi instead. It was at this point that the group also added the second thermocoupling, located closer to the heat gun (hereafter the near reading).

Test #4: 20 mL Water in "Harold"
The group often referenced the Properties of Saturated Steam Table to see if the water was behaving as expected, which also helped to determine how accurate measurements were.
Finally, with all of the stupid mistakes out of the way, and a pressure gauge more readily able to measure the amount of pressure the heat pipe would be dealing with, the group began their fourth trial of 20 mL of water. Because of the previous difficulties, and the fact that the heat pipe had in all likelihood lost water overnight and during the change of gauges, this trial was not timed. Still, observations could be named, if not charted and graphed. The temperature rose steadily. There was a first pressure pause at 6.5 psi (on the gauge, which begins its measurement at 1 atm or 14.696 psi) and around 220°F. The group found a Properties of Saturated Steam Table lying around in the basement, and had a good time referencing it as they worked with the heat pipe. The temperature continued rising, but paused again at 240°F. The group had some concerns and attempted to troubleshoot during this trial. To rid the system of air bubbles, the venting valve at the top was opened, and a blowtorch was used to add more heat to the bottom of the heat pipe, boiling the water inside and venting steam through the top. The slower speed of the heat rising compared to the previous night's trials led the group to properly evacuate the heat pipe and add fresh water. While this was happening, a plain copper tube of about the same length of the heat pipe was added, and both thermocouplings were transferred sot that the group could establish a baseline test of the heating speed of copper. 

Test #5: Plain Length of Copper Tube
Above is the initial copper test where the copper tubing is not isolated from the vice.
During the first trial of plain copper tubing, the data indicated that there was a drop in temperature at the beginning that didn't quite make sense until someone pointed out that the vice holding the copper was made of metal and could work as a heat sink. The group decided to run through 10 minutes worth of temperature data anyway, but run a second test to see if it made any sort of significant difference in results. The temperature rose slowly compared to even the more disappointing heat pipe tests, which was encouraging to say the least. 
Time Copper Near Copper Far ΔT Copper
30 112 76 36
60 160 74.8 85.2
90 187 74.6 112.4
120 205 74.6 130.4
150 218 74.4 143.6
180 225 75 150
210 230 75 155
240 234 75.4 158.6
270 237 76 161
300 238 76.8 161.2
330 239 77 162
360 240 77.4 162.6
390 241 77.6 163.4
420 241 77.8 163.2
450 241 78 163
480 241 78.2 162.8
510 241 78.4 162.6
540 241 78.8 162.2
570 245 79 166
600 246 79 167
 
 
 

Test #6: Copper Baseline Take II (isolated from the vice using small pieces of oak)
The second copper trial went smoothly. The heat gun was putting out somewhere between 600°F and 700°F. The group once again cut the test off at 10 minutes, feeling that there was enough information available to create an accurate depiction of the heat transfer properties of copper tubing by itself, isolated from the system. At the 10 minute mark, the bottom of the system was at nearly 300°F, while the upper thermocoupling read only 99.4°F. Even with the earlier heat pipe tests going disappointingly, they were much faster, and hotter than the copper alone. The temperature increased very steadily, almost linearly. Even isolated, there was a temperature dip in the beginning of the experiment. The group was not positive about why. Perhaps the pipe was still cooling from the last experiment, or the wood soaked up some of the initial heat. 
Time Copper Near Copper Far ΔT Copper
30 118 72.8 45.2
60 178 72.6 105.4
90 217 72.8 144.2
120 240 73.4 166.6
150 255 75 180
180 268 77 191
210 275 79.4 195.6
240 280 81.8 198.2
270 285 84.4 200.6
300 287 86.2 200.8
330 291 88 203
360 293 90 203
390 294 92 202
420 296 93.6 202.4
450 295 94.8 200.2
480 297 95.8 201.2
510 298 96.8 201.2
540 298 97.8 200.2
570 299 98.8 200.2
600 300 99.4 200.6
  
 
 






Test #7: 20mL (new) Water in "Harold"
After the previous tests, the group decided to have a fresh start, and drained the heat pipe and added fresh water. The test went well this time. Once again, the test was cut off at 30 psi instead of any time constraint, because of concerns about the solder joints failing and spewing hot water all across the room. It took about 00:10:30 to reach the cut-off point of 30 psi, and the temperature at the top of the heat pipe at that point was 270°F. According to the saturated steam tables, pressure should have been at about 41.85 psi, or according to our gauge 27.15 psi above 1 atm. This was about where  we were, so all in all not a bad trial.
Time Water Near Water Far ΔT Water
30 102 75.4 26.6
60 163 75.4 87.6
90 184 75.8 108.2
120 197 138.6 58.4
150 205 185.4 19.6
180 211 200.4 10.6
210 214 208.8 5.2
240 219 213.6 5.4
270 222 218.2 3.8
300 226 221.8 4.2
330 229 225.2 3.8
360 234 229.8 4.2
390 240 235 5
420 243 238.8 4.2
450 246 244.4 1.6
480 253 249.6 3.4
510 258 254 4
540 262 258 4
570 266 262.8 3.2
600 271 267 4
630 274 270.6 3.4
  
 
 
 

Test #8: 20 mL Methanol in "Harold"
There were concerns this round of testing, because during the bleeding process, the pressure spiked to 5 psi within 30 seconds of exposure to the blowtorch, so the process had to be watched much more carefully. The heat transfer was better than copper alone, and a little bit quicker than water, but the pressure rose so quickly that the trial had to be stopped in less than 10 minutes, and the temperature maxed out at 201.8°F at the top of the pipe and 216°F near the heat source, which is considerably lower than the 270°F that water reached during the trial. By the end of the test, we decided as a group to not use methanol in the final product.
Karen donned the only safety mask, because she was the closest to the heat pipe.

Time  Methanol Near Methanol Far ΔT Methanol
0 103 69 34
30 146 70 76
60 155 129.8 25.2
90 167 154.6 12.4
120 173 164.4 8.6
150 177 168 9
180 181 171.2 9.8
210 186 175.4 10.6
240 193 181.2 11.8
270 201 188.2 12.8
300 205 195 10
330 216 201.8 14.2

 
 
 
Test #9: 20 mL Acetone in "Harold" 
Acetone also rose in pressure with impressive speed, which was a bit nerve-wracking. At about 30 psi, the trial was stopped. The temperature at the farther thermocoupling was 192.4°F, which was also much lower than the maximum heat for the 20mL of water. In addition to this, both acetone and methanol are fluids that you really don't want to accidentally spill into your ham, so at this point the group made a decision to use water in the final product instead of either of these two fluids. Someone suggested that the group purchase some 25/75% mixture of ammonia and water, as that is what's used in more industrial settings, but the group is unsure of whether or not they will be doing that. 
 
Time Temp Near Temp Far ΔT 
0 68 70.4 -2.4
30 106 70.2 35.8
60 131 105.6 25.4
90 142 132 10
120 152 142 10
150 163 152.4 10.6
180 175 163 12
210 188 170.4 17.6
240 196 177.8 18.2
270 206 185.6 20.4
300 216 192.4 23.6
 
 
 
 
Trial #10: 25 mL Water in "Harold"
The group had really only guessed at the 20mL, assuming that it was a decent trial amount as it filled the majority of the "well" at the bottom of the heat pipe (the name we used for the wider, evaporator end of the pipe). The 25mL trial went swimmingly. It was the first trial to actually have a higher temperature at the top of the pipe than the bottom of the pipe, which was pretty exciting. 

Time Temp. Near Temp. Far ΔT
0 85.0 84 1.0
30 110.0 84 26.0
60 133.8 83 50.8
90 151.0 83 68.0
120 161.1 92 69.1
150 173.8 149 24.8
180 180.8 168 12.8
210 186.2 182 4.2
240 191.8 176 15.8
270 195.0 190 5.0
300 201.2 197 4.2
330 208.6 206 2.6
360 214.8 213 1.8
390 219.8 220 -0.2
420 223.4 225 -1.6
450 227.2 229 -1.8
480 230.4 232 -1.6
510 233.4 235 -1.6
540 236.4 238 -1.6
570 238.8 241 -2.2
600 242.2 244 -1.8
630 245.0 247 -2.0
660 247.6 250 -2.4
690 250.6 253 -2.4
720 253.4 254 -0.6
750 255.4 257 -1.6
780 257.6 259 -1.4
810 259.8 261 -1.2
840 261.8 262 -0.2
870 263.6 264 -0.4
900 265.2 268 -2.8
930 266.8 268 -1.2
 
 
 
 
 

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